| -- End Ad Box ---> | | | | cellulose and reduced its strength. All of these led |
| Historically, most of society’s writings and | | | | to diminution of paper properties. Fortunately, |
| visual images have been recorded on paper. | | | | bleaching processes have totally significantly over |
| However, paper is an organic material and is | | | | the past few decades and the chlorination and |
| subject to deterioration caused by chemical, | | | | hypochlorite steps are no longer used resulting in |
| physical and biological agents. While documents on | | | | less damage is done to resulting fiber. |
| paper several hundreds of years old have | | | | The strength of paper results from a combination |
| endured, most paper manufactured in the last | | | | of factors. The most important is the condition of |
| two hundred years has a limited storage life due | | | | cellulose, in particular chain length. Cellulose is made |
| primarily to acidity induced as part of paper | | | | up of repeating units of glucose monomers and |
| manufacturing processes used during that time | | | | the number of glucose units present provides a |
| period. Exposure to acidic air pollutants also | | | | measure of degree of polymerization (DP). In |
| contributes to paper degradation. | | | | native cellulose from wood DP is about 10,000. |
| Chemically this degradation is a result of acid | | | | Depending on the nature of the pulping and |
| hydrolysis of the cellulose polymers which are | | | | bleaching, the DP of processed cellulose falls to a |
| themselves responsible for the intrinsic strength | | | | range of 600 — 1100. |
| found in paper sheets. The hydrolysis reaction are | | | | After this reduction the paper fibers are still quite |
| also autocatalytic since they produce additional | | | | strong, but fiber strength is highly dependent upon |
| acid products which themselves further increase | | | | retaining this DP and acids break cellulose bonds |
| paper acidity and accelerate degradation occurring. | | | | randomly often cutting the cellulose polymer in |
| Since untreated paper is too absorbent for the | | | | central regions. These attacks drastically reduce |
| application of inks, hydrophobic fillers also called | | | | the DP of cellulose and quickly weaken the fibers. |
| sizings are added to paper surfaces as part of | | | | Alkalis also attack cellulose, but by a different |
| the manufacturing process which can also have an | | | | mechanism, in which only end units are removed |
| impact on paper permanence. Sizing impacts | | | | (end peeling) so that alkaline degradation has much |
| absorption of liquids to prevent feathering of inks | | | | less effect on reducing DP (Bristow and Kolseth, |
| and dyes and to provide a crisp image. | | | | 1986) |
| Paper made before the 19th century was often | | | | Some low quality papers such as groundwood for |
| made by hand from linen and cotton rag materials | | | | newsprint also contain high amounts of lignin. |
| which are excellent sources of high cellulose, long | | | | Lignin contains phenolic entities sensitive to light |
| fibers. Gelatin, from animal hides, was used to size | | | | which develop chromophores or conjugated |
| such papers and because the resulting papers | | | | double bonds in the chemical structure which can |
| were neutral to only slightly alkaline they had very | | | | absorb light in the visible range. This makes paper |
| good storage properties. The paper machine | | | | containing high amounts of lignin very prone to |
| appeared at the end of the 18th century, and as | | | | discoloration or yellowing. While there is no doubt |
| the demand for paper outpaced sources of | | | | that lignin in paper contributes to its discoloration, |
| available gelatin, cotton rags and linen, wood fiber | | | | there is little evidence to show that paper |
| took the place of cotton and linen. However, | | | | containing lignin loses strength faster than paper |
| wood has shorter fibers and lower cellulose | | | | of similar quality without lignin (Luner, 1988). |
| content along with lignin so that chemical methods | | | | However, standard specifications for durable |
| had to be developed to free fibers from wood | | | | paper allow no more than 1% lignin, for papers |
| and other plant matter to supply the increasing | | | | used in archives, libraries, and other permanent |
| amounts of paper furnish needed. Mechanical | | | | records. |
| action [“beating”] to soften and bleaching to | | | | In addition to the acid nature inherent in paper and |
| whiten these new materials yielded pulps that | | | | the exposure to acidic air pollutants, it is now |
| could be laid down by machine as a sheet with | | | | known that exposure of stable or acid free paper |
| subsequent drying to form paper. | | | | to acidic books and papers — as in a library |
| Gelatin was replaced in the early 1800s with rosin | | | | or archive — will lead to deterioration of |
| which was mainly abietic acid isolated from pine | | | | such seemingly stable documents stored within |
| resin. Alum (papermaker’s alum or | | | | the same collections (Smith, 1999). Other threats |
| aluminum sulfate) was used to precipitate the | | | | to permanence include those from water and fire |
| rosin onto paper forming an alum/rosin sizing. | | | | damage, theft, and vandalism or biological agents. |
| Aluminum sulfate reacts with water - and | | | | These are problems while not inherently present |
| produces sulfuric acid — and production of | | | | with paper materials have been addressed in |
| paper on the paper machine demanded additional | | | | depth by the Northeast Document Conservation |
| alum, so papermakers often used the salt in | | | | Center (NDCC, 1999). |
| excess. The industrial revolution added outside | | | | Because of its importance to society, the |
| factors such as air pollution and acidic oxides of | | | | permanence of paper is addressed in a significant |
| nitrogen or sulfur and ozone to the environment. | | | | and growing literature much of which has been |
| Early bleaching processes using chlorine and | | | | generated by the community of archivists and |
| hypochlorites, strong oxidizers, also degraded the | | | | librarians. |